In-situ Characterization of Heterogeneous Catalysts

ISBN: 9781118000168 出版年：2013 页码：490 Jose A Rodriguez Jonathan C Hanson Wiley

CONTRIBUTORS vii Introduction: Goals and Challenges for the In-situ Characterization of Heterogeneous Catalysts 1 Jose A. Rodriguez, Jonathan C. Hanson, and Peter J. Chupas 1 QEXAFS in Catalysis Research: Principles, Data Analysis, and Applications 23 Anatoly I. Frenkel, Syed Khalid, Jonathan C. Hanson, and Maarten Nachtegaal 2 Spatially Resolved X-ray Absorption Spectroscopy 49 Christian G. Schroer and Jan-Dierk Grunwaldt 3 Energy-Dispersive EXAFS: Principles and Application in Heterogeneous Catalysis 75 Mark A. Newton and Andrew J. Dent 4 In-situ Powder X-ray Diffraction in Heterogeneous Catalysis 121 Jonathan Hanson and Poul Norby 5 Pair Distribution Function Analysis of High-Energy X-ray Scattering Data 147 Karena W. Chapman and Peter J. Chupas 6 Neutron Scattering for In-situ Characterization of Heterogeneous Catalysis 169 Ashfi a Huq and Wei-Ren Chen 7 Visualization of Surface Structures of Heterogeneous Catalysts under Reaction Conditions or during Catalysis with High-Pressure Scanning Tunneling Microscopy 191 Luan Nguyen, Shiran Zhang, Yingchun Ye, Yuan Zhu, Lei Wang, and Franklin (Feng) Tao 8 In-situ Infrared Spectroscopy on Model Catalysts 209 Kumudu Mudiyanselage and Dario J. Stacchiola 9 Infrared Spectroscopy on Powder Catalysts 241 Eli Stavitski 10 Structural Characterization of Catalysts by Operando Raman Spectroscopy 267 Gerhard Mestl and Miguel A. Banares 11 In-situ Electron Paramagnetic Resonance of Powder Catalysts 293 Angelika Bruckner 12 Application of Ambient-Pressure X-ray Photoelectron Spectroscopy for the In-situ Investigation of Heterogeneous Catalytic Reactions 315 David E. Starr, Hendrik Bluhm, Zhi Liu, Axel Knop-Gericke, and Michael Havecker 13 Combined X-ray Diffraction and Absorption Spectroscopy in Catalysis Research: Techniques and Applications 345 Anatoly I. Frenkel and Jonathan C. Hanson 14 Combining Infrared Spectroscopy with X-ray Techniques for Interrogating Heterogeneous Catalysts 369 Mark A. Newton and Marcos Fernandez-Garcia 15 XRD Raman and Modulation Excitation Spectroscopy 411 Wouter van Beek, Atsushi Urakawa, and Marco Milanesio 16 Catalyst Imaging Using Synchrotron-Based Multitechnique Approaches 441 Andrew M. Beale, Javier Ruiz-Martinez, and Bert M. Weckhuysen INDEX 475